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Visualization and quantification of capillary drainage in the pore space of laminated sandstone by a porous plate method using differential imaging X-ray microtomography

机译:利用差分成像X射线显微断层多孔板法对层状砂岩孔隙中毛细管引流进行可视化和定量分析

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摘要

The experimental determination of capillary pressure drainage curves at the pore scale is of vital importance for the mapping of reservoir fluid distribution. To fully characterize capillary drainage in a complex pore space, we design a differential imaging-based porous plate (DIPP) method using X-ray micro- tomography. For an exemplar mm-scale laminated sandstone microcore with a porous plate, we quantify the displacement from resolvable macropores and subresolution micropores. Nitrogen (N 2 ) was injected as the nonwetting phase at a constant pressure while the porous plate prevented its escape. The measured porosity and capillary pressure at the imaged saturations agree well with helium measurements and experi- ments on larger core samples, while providing a pore-scale explanation of the fluid distribution. We observed that the majority of the brine was displaced by N 2 in macropores at low capillary pressures, fol- lowed by a further brine displacement in micropores when capillary pressure increases. Furthermore, we were able to discern that brine predominantly remained within the subresolution micropores, such as regions of fine lamination. The capillary pressure curve for pressures ranging from 0 to 1151 kPa is provided from the image analysis compares well with the conventional porous plate method for a cm-scale core but was conducted over a period of 10 days rather than up to few months with the conventional porous plate method. Overall, we demonstrate the capability of our method to provide quantitative information on two- phase saturation in heterogeneous core samples for a wide range of capillary pressures even at scales smaller than the micro-CT resolution
机译:在孔隙尺度上实验确定毛细管压力排放曲线对于绘制储层流体分布至关重要。为了充分表征复杂孔隙空间中的毛细血管引流,我们设计了使用X射线显微断层扫描的基于差分成像的多孔板(DIPP)方法。对于具有多孔板的示例性毫米级层压砂岩微芯,我们量化了可分辨大孔和亚分辨率微孔的位移。以恒定压力注入氮气(N 2)作为非润湿相,同时多孔板阻止其逸出。在成像饱和度下测得的孔隙度和毛细压力与氦气的测量结果以及较大岩心样品上的实验结果非常吻合,同时提供了孔隙尺度解释了流体分布。我们观察到,在低毛细管压力下,大孔中的大部分盐水被N 2置换,随后在毛细管压力增加时,微孔中的盐水进一步置换。此外,我们能够辨别出盐水主要保留在亚分辨率微孔内,例如精细层压区域。由图像分析提供的压力范围为0到1151 kPa的毛细管压力曲线与常规的多孔板方法(厘米级芯)相比具有很好的对比性,但使用的时间为10天,而不是常规的长达几个月多孔板法。总的来说,我们证明了我们的方法能够为各种毛细管压力提供均质岩心样品中两相饱和度的定量信息,即使尺度小于微型CT分辨率

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